Nuclear Magnetic Resonance Facility
Alex Greenwood
The NMR facility in the Chemistry department currently houses three solution NMR instruments ranging from 400-500 MHz. These include two walk-up Bruker 400s (an AVANCE NEO and an AVANCE I) with Z-Grad BBFO (Z-Gradient Broadband and Fluorine Observe) ATM (Automatic Tune and Match) probes and SampleXpress Lite automatic sample changers, and a Bruker DMX-500 with Z-Grad triple and double resonance probes. The NMR facility is capable of proton, carbon-13 and other multi-nuclear NMR in one, two, and three dimensions. Common experiments include HSQC (Heteronuclear Single-Quantum Coherence), COSY (COrrelated SpectroscopY), NOESY (Nuclear Overhauser Enhancement SpectroscopY), and DOSY (Diffusion-Ordered SpectroscopY).
Location & Hours:
The Chemistry NMR facility is located in Crosley Tower, rooms 123 and 108. Walk-up instruments are available 24/7 for trained users.
-
SENSORS Nicolet FTIR spectrometer & microscope unassisted
Cost:Request Information$40.00/hr
-
SENSORS (ESEM) Environmental Scanning Electron Microscope assisted
Cost:Request Information$90.00/hr
-
SENSORS INSTRUMENTS GROUP 1 UNASSISTED (see instruments below)
Cost:Request Information$10.00/hr
-
SENSORS Veeco multimode scanning probe microscope
Cost:Request Information$40.00/hr
-
SENSORS INSTRUMENTS GROUP 2 UNASSISTED (see instruments below)
Cost:Request Information$30.00/hr
-
X-Ray Data Set Academic/SAMPLE
Cost:Request Information$100.00/hr
-
X-Ray Setup Academic/SAMPLE
Cost:Request Information$15.00/hr
-
X-Ray Unit Cell Only Academic/SAMPLE
Cost:Request Information$50.00/hr
-
X-ray synchtron /SAMPLE (formerly Beamline consortium time/SAMPLE)
Cost:Request Information$50.00/hr
-
NMR 500 1-8 HRS (1/2/ HR MINIMUM)/hour
Cost:Request Information$8.00/hr
-
NMR 500 9-24 HRS/hour
Cost:Request Information$6.00/hr
-
NMR 500 >24 HRS/hour
Cost:Request Information$4.00/hr
-
NMR AV400, AMX400 1-8 HRS (1/2/ HR MINIMUM)/hour
Cost:Request Information$6.00/hr
-
NMR AV400, AMX400 9-24 HRS/hour
Cost:Request Information$5.00/hr
-
NMR AV400, AMX400 >24 HRS/hour
Cost:Request Information$3.00/hr
-
ICP-MS Academic Qualitative Analysis/hour
Cost:Request Information$38.00/hr
-
ICP-MS Academic Quantitative Analysis/hour
Cost:Request Information$38.00/hr
-
ICP-MS Academic Quantitative Setup fee/sample
Cost:Request Information$50.00/hr
-
ICP-MS Academic Qualitative Analysis Set Up Fee/sample
Cost:Request Information$38.00/hr
-
ICP-MS Academic Qualitative Sample Prep/hour
Cost:Request Information$38.00/hr
-
ICP-MS Academic Quantitative Analysis Sample Prep/hour
Cost:Request Information$38.00/hr
-
ICP-MS Academic QA Time Resolved Set Up fee/sample run
Cost:Request Information$109.00/hr
-
ICP-MS Academic QA Time Resolved/sample
Cost:Request Information$38.00/hr
-
ICP-MS Academic QA Time Resolved per hour/if cheaper than per sample
Cost:Request Information$109.00/hr
-
ICP-MS Academic QA Time Resolved Sample prep/hour
Cost:Request Information$38.00/hr
-
MASSSPEC General MS/hour
Cost:Request Information$80.00/hr
-
MASSSPEC MS ANALYSIS (<1000 Da) rate/sample
Cost:Request Information$25.00/hr
-
MASSSPEC MS ANALYSIS (>1000 Da) rate/sample
Cost:Request Information$35.00/hr
-
MASSSPEC GC-MS per injection
Cost:Request Information$120.00/hr
-
MASSSPEC LC-MS per injection
Cost:Request Information$25.00/hr
-
MASSSPEC GC-MS self operated/hour (1/2 hour minimun)
Cost:Request Information$15.00/hr
-
MASSSPEC LTQ-FTMS SURCHARGE/SAMPLE
Cost:Request Information$2.00/hr